# US 10,502,670 B2 · Temperature compensated density viscosity sensor having a resonant sensing element > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 10,502,670 B2 - Document ID: US10502670B2 - Status: Granted - Kind: B2 - Application number: 15/566,675 - Filed: 2016-04-14 - Published: 2019-01-03 - Granted: 2019-12-10 - Earliest claimed: 2015-04-14 - Assignees: Rheonics GmbH - Applicants: Rheonics GmbH - Inventors: Joseph H. Goodbread; Sunil Kumar; Klaus Haeusler; Bernhard Zybach - Web page: https://patentgrep.com/patent/US10502670B2 ## CPC - G01N 9/002: {using variation of the resonant frequency of an element vibrating in contact with the material submitted to analysis (G01N9/34 takes precedence)} - G01N 11/10: by moving a body within the material - G01N 11/16: by measuring damping effect upon oscillatory body - G01N 11/162: {Oscillations being torsional, e.g. produced by rotating bodies} - G01N 29/036: by measuring frequency or resonance of acoustic waves - G01N 2009/006: {vibrating tube, tuning fork} - G01N 2291/02818: Density, viscosity - G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q) ## Abstract A fluid density measurement device that includes a housing, defining a chamber and an aperture; a resonator having length that is at least 5 times greater than its smallest diameter and having a longitudinal axis and a nodal plane, transverse to the longitudinal axis. The resonator further includes a tube having a first end and a second end; a second-end closure, closing the second end; and a drive rod centrally attached to the second-end closure and extending to the tube first end. Further, the device includes a resonator transducer assembly and the resonator is sealingly joined to the aperture at the nodal plane, so that an enclosed portion extends into the chamber and an exposed portion extends outside of the chamber, and wherein the chamber tends to assume the temperature of the exposed resonator portion, causing the resonator to be isothermal. ## Claims ### Claim 1 A method of measuring density of a target fluid, comprising the steps (a) providing a fluid density measurement device, including: (i) a housing, defining a chamber and an aperture; (ii) a resonator having length that is at least 5 times greater than its smallest diameter and having a longitudinal axis and nodal plane, transverse to said longitudinal axis, and that includes a tube having a first end and a second end and being closed at said second end by a second-end closure, and being attached to said housing at said nodal plane, which is sealingly joined to said aperture, blocking fluid ingress, and so that an enclosed resonator portion extends into said chamber and an exposed resonator portion extends outside of said chamber; and further including a drive rod centrally attached to said second-end closure and extending into said enclosed resonator portion; (iii) wherein said second-end closure includes a fluid end mass that would define a non-round shape on a plane cutting through said end mass transversely to said longitudinal axis and wherein said resonator is driven to vibrate torsionally about its longitudinal axis, and said target fluid is displaced by resultant rotational vibration of said end mass; and (iv) a transducer assembly; and (b) placing said exposed portion of said resonator in said target fluid; (c) placing and maintaining said resonator into an isothermal state; (d) using said transducer assembly to excite said resonator such that said exposed resonator portion vibrates perpendicularly to a portion of its own surface and to sense resultant resonator vibrations; and (e) analyzing said resultant vibrations to determine density of said target fluid. ### Claim 2 (depends on 1) The method of claim 1, wherein said drive rod is in form of a tube. ### Claim 3 (depends on 1) The method of claim 1, wherein said fluid end mass defines a flat surface, extending in parallel to said longitudinal axis. ### Claim 4 (depends on 1) The method of claim 1, wherein at least one fin extends from said end mass, thereby causing more displacement of said target fluid by rotational vibration of said end mass. ### Claim 5 (depends on 4) The method of claim 4, wherein a plurality of fins extends from said end mass, said four fins being spaced equally about said end mass. ### Claim 6 (depends on 1) The method of claim 1 wherein said drive rod bears a magnet that together with a nearby electromagnet assembly mounted on said housing forms at least a part of said resonator exciting and sensing assembly. ### Claim 7 (depends on 1) The method of claim 1, wherein said housing is fluid impermeable and wherein both said housing and said exposed resonator portion are placed in said target fluid, so that said chamber and said enclosed resonator portion tend to assume the temperature of said target fluid and said exposed resonator portion, thereby placing and maintaining said resonator into an isothermal state. ### Claim 8 (depends on 1) The method of claim 1, wherein said housing is highly thermally insulating, causing said chamber to be adiabatic, so that said step of placing said exposed resonator portion into said target fluid causes said enclosed resonator portion to approach the temperature of said target fluid, thereby placing said resonator into an isothermal state. ### Claim 9 (depends on 1) The method of claim 1, wherein said measurement device further includes a temperature sensor located in said exposed resonator portion, and also further includes a temperature control element positioned to control temperature of said chamber and being responsive to said temperature sensor to control temperature of said chamber and thereby said enclosed resonator portion to equal that of said exposed resonator portion, so that said resonator is placed and maintained in an isothermal state. ### Claim 10 (depends on 1) The method of claim 1, wherein said tube extends into said chamber and is closed at its first end by a first end closure that includes an element of said transducer assembly. ### Claim 11 (depends on 10) The method of claim 10, wherein said element of said transducer assembly is a permanent magnet and wherein said transducer assembly further includes an electrical coil assembly, adapted to drive said permanent magnet and to sense its movement. ### Claim 12 A fluid density measurement device, including: (a) a housing, defining a chamber and an aperture; (b) a resonator having length that is at least 4 times greater than its smallest diameter and having a longitudinal axis and nodal plane, transverse to said longitudinal axis, and that includes: (i) a tube having a first end and a second end; (ii) a second-end closure, closing said second end; and (c) a drive rod centrally attached to said second-end closure and extending to said tube first end; (d) a resonator transducer assembly; (e) wherein said resonator is sealingly joined to said aperture at said nodal plane, blocking fluid ingress, and so that an enclosed resonator portion extends into said chamber and an exposed resonator portion extends outside of said chamber, and wherein said resonator transducer assembly drives said resonator such that said exposed resonator portion vibrates perpendicularly to a portion of its own surface; and (f) wherein said measurement device further includes a temperature sensor located in said exposed resonator portion, and also further includes a temperature control element positioned to control temperature of said chamber and being responsive to said temperature sensor to control temperature of said chamber and thereby said enclosed resonator portion to equal that of said exposed resonator portion, so that said resonator is placed and maintained in an isothermal state. ### Claim 13 (depends on 12) The device of claim 12, wherein said housing is fluid impermeable and wherein both said housing and said exposed resonator portion are placed in said target fluid, so that said chamber and said enclosed resonator portion tend to assume the temperature of said target fluid and said exposed resonator portion, thereby further helping to place and maintaining said resonator into an isothermal state. ### Claim 14 (depends on 12) The device of claim 12, wherein said housing is highly thermally insulating, causing said chamber to be adiabatic, so that said step of placing said exposed resonator portion into said target fluid causes said enclosed resonator portion to approach the temperature of said target fluid, thereby further helping to place said resonator into an isothermal state. ### Claim 15 (depends on 12) The device of claim 12, wherein said tube extends into said chamber and is closed at its first end by a first end closure that includes an element of said transducer assembly. ### Claim 16 (depends on 15) The device of claim 15, wherein said element of said transducer assembly is a permanent magnet and wherein said transducer assembly further includes an electrical coil assembly, adapted to drive said permanent magnet and to sense its movement. ### Claim 17 A method of measuring density of a target fluid, comprising the steps of: (a) providing a fluid density measurement device, including: (i) a housing, defining a chamber and an aperture; (ii) a resonator having length that is at least 5 times greater than its smallest diameter and having a longitudinal axis and nodal plane, transverse to said longitudinal axis, and that includes a tube having a first end and a second end and being closed at said second end by a second-end closure, and being attached to said housing at said nodal plane, which is sealingly joined to said aperture, blocking fluid ingress, and so that an enclosed resonator portion extends into said chamber and an exposed resonator portion extends outside of said chamber; and further including a drive rod centrally attached to said second-end wall and extending into said enclosed resonator portion; (iii) a transducer assembly; and (iv) a first temperature measurement device in said enclosed portion and a second temperature measurement device in said exposed portion; (b) placing said exposed portion of said resonator in said target fluid; (c) using said transducer assembly to excite said resonator such that said exposed resonator portion vibrates perpendicularly to a portion of its own surface; and (d) analyzing said resultant vibrations and said measurements of said first temperature sensor and said second temperature sensor to determine density of said target fluid. ### Claim 18 A method of measuring density of a target fluid, comprising the steps (a) providing a fluid density measurement device, including: (i) a housing, defining a chamber and an aperture; (ii) a resonator having length that is at least 5 times greater than its smallest diameter and having a longitudinal axis and nodal plane, transverse to said longitudinal axis, and that includes a tube having a first end and a second end and being closed at said second end by a second-end closure, and being attached to said housing at said nodal plane, which is sealingly joined to said aperture, blocking fluid ingress, and so that an enclosed resonator portion extends into said chamber and an exposed resonator portion extends outside of said chamber; and further including a drive rod centrally attached to said second-end closure and extending into said enclosed resonator portion; (iii) a transducer assembly; (iv) a temperature sensor located in said exposed resonator portion; and (v) a temperature control element positioned to control temperature of said chamber and being responsive to said temperature sensor to control temperature of said chamber and thereby said enclosed resonator portion to equal that of said exposed resonator portion, so that said resonator is placed and maintained in an isothermal state; and (b) placing said exposed portion of said resonator in said target fluid; (c) placing and maintaining said resonator into an isothermal state; (d) using said transducer assembly to excite said resonator such that said exposed resonator portion vibrates perpendicularly to a portion of its own surface and to sense resultant resonator vibrations; and (e) analyzing said resultant vibrations to determine density of said target fluid.