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US 10,464,853 B2Granted
Source of phosphate for agriculture and the food industry
AssigneeEcophos S.A.
InventorMohamed Takhim
Life of this patent
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Abstract
A source of phosphate for agriculture and food industry comprises a phosphate salt in solid form of formula Mn(HPO4)y.zH2O in which M is Na, K, NH4, n=2, and y=1; or M is Ca, n=1, y=1; or M is Al or Fe, n=2, y=3; and in which z is 0, 1 or 2, wherein said phosphate salt has a phosphate content expressed as a P2O5 content of between 30 and 50% by weight of the phosphate salt, and it has a cadmium content lower than 0.40 ppm.
Claims19
A method comprising:
- a) digesting a phosphate source using a first aqueous solution of hydrochloric acid to form an attack liquor consisting of an aqueous phase comprising phosphate ions and chloride ions in solution, and a first insoluble solid phase containing impurities,
- b) separating the aqueous phase comprising phosphate and chloride ions in solution from the first insoluble solid phase containing impurities,
- c) neutralizing said aqueous phase comprising phosphate ions and chloride ions in solution at a pH sufficient to form an aqueous medium comprising chloride ions and to precipitate the phosphate ions in the form of a phosphate salt,
- d) separating said aqueous medium comprising chloride ions from said phosphate salt,
- wherein a) and b) are performed at a temperature between 50° C. and 70° C. for a duration less than two hours and wherein said first aqueous solution of hydrochloric acid has an HCl concentration of 12-15% by weight, and further wherein the neutralization carried out in c) takes less than one hour.
2 more elements
Dependencies are inferred from the claim text.