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US 10,377,907 B2Granted
Substrate with a superhydrophobic coating and a method of fabricating thereof
AssigneeKing Fahd University of Petroleum and Minerals
InventorsAbuduliken Bake, Nesar Merah
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Abstract
A substrate with a superhydrophobic coating, wherein the superhydrophobic coating includes a binding layer disposed on the substrate, and a hydrophobic layer disposed on the binding layer, wherein the hydrophobic layer includes perfluoroalkyl-functionalized silica nanoparticles, and a method of fabricating the substrate with the superhydrophobic coating. Various combinations of embodiments of the substrate with the superhydrophobic coating and the method of fabricating thereof are provided.
Claims16
A method of forming a superhydrophobic coating, comprising:
- mixing a solution comprising an alkyl alkoxysilane, a glycidyl-containing alkoxysilane, an alcohol, ammonium hydroxide, and water for 20 to 60 minutes to form a mixture and applying the mixture onto a substrate;
- heating the substrate and the mixture applied thereon, wherein the substrate is functionalized with the alkyl alkoxysilane and the glycidyl-containing alkoxysilane, thereby forming a coated substrate comprising a binding layer on the substrate;
- applying a suspension comprising perfluoroalkyl-functionalized silica nanoparticles onto the coated substrate to form a hydrophobic layer on the binding layer, thereby forming the superhydrophobic coating;
- and
- annealing the substrate with the superhydrophobic coating at a temperature in the range of 100° C. to 300° C. for no more than 2 hours,
- wherein the alkyl alkoxysilane is selected from the group consisting of methytrimethoxysilane, methyltriethoxysilane, ethyltrimethoxysilane, trimethylethoxysilane, and dimethyldiethoxysilane, and
- wherein the glycidyl-containing alkoxysilane is (3-glycidyloxypropyl) trimethoxysilane.
4 more elements
Dependencies are inferred from the claim text.