Process for preparing tris[3-(alkoxysilyl)propyl]isocyanurates
AssigneeEvonik Degussa GmbH
InventorsPhilipp Albert, Eckhard Just
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Abstract
A process can prepare an isocyanurate compound by hydrosilylation. The compound is a tris[3-(trialkoxysilyl)propyl] isocyanurate, a tris[3-(alkyldialkoxysilyl)propyl] isocyanurate, and/or a tris[3-(dialkylalkoxysilyl)propyl] isocyanurate. The process includes (A) preparing a mixture of at least one carboxylic acid, a platinum catalyst, and 1,3,5-triallyl-1,3,5-triazine-2,4,6(1H,3H,5H)-trione; (B) heating the mixture to a temperature in the range of 40 to 140° C.; (C) adding at least one H-silane among a hydrotrialkoxysilane, a hydroalkyldialkoxysilane, and a hydrodialkylalkoxysilane to the mixture; (D) adding at least one alcohol to the mixture prepared in step (C); and (E) isolating the isocyanurate compound.
Claims17
A process for preparing a tris[3-(alkoxysilyl)propyl]isocyanurate of the formula:
- comprising the following steps:
- (A) preparing a mixture comprising at least one carboxylic acid, a platinum catalyst and 1,3,5-triallyl-1,3,5-triazine-2,4,6(1H,3H,5H)-trione of the formula:
- (B) heating the mixture prepared in step (A) to a temperature in the range of 40° C.-140° C.;
- (C) adding a hydrosilane of the formula:
- (CH3CH2O)3SiH,
- to the mixture prepared in step (B);
- (D) adding at least one alcohol to the mixture prepared in step (C);
- and
- (E) isolating the tris[3-(alkoxysilyl)propyl]isocyanurate of the formula above.
Dependencies are inferred from the claim text.