# US 10,371,654 B2 · System and method for a nondestructive on-line testing of samples

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- Number: US 10,371,654 B2
- Document ID: US10371654B2
- Status: Granted
- Kind: B2
- Application number: 15/290,609
- Filed: 2016-10-11
- Published: 2017-02-02
- Granted: 2019-08-06
- Earliest claimed: 2006-08-21
- Assignees: Aspect Ai Ltd.
- Applicants: Aspect Al Ltd.
- Inventors: Uri Rapoport
- Web page: https://patentgrep.com/patent/US10371654B2

## CPC

- G01N 24/085: {Analysis of materials for the purpose of controlling industrial production systems}
- G01N 22/04: Investigating moisture content
- G01N 27/023: {where the material is placed in the field of a coil}
- G01N 33/02: Food
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)

## Abstract

An MRI-free non-destructive on-line system for detecting a presence of a material in a sample. The system includes a flow conduit encompassed by a tunable RF coil and having an input duct and an output duct; a flow of the sample through the flow conduit; a signal detector that detects frequency-dependent output signals as a function of a frequency variation of the RF tunable coil within a frequency range of an RF resonant frequency of a standard sample of the substance; and a processing unit.

## Claims

### Claim 1

A non-destructive on-line method for detecting a material in a sample of a substance comprising:
providing a flow conduit encompassed by the tunable radio frequency (RF) coil;
providing a flow of the sample through the flow conduit;
detecting frequency-dependent output signals as a function of a frequency variation of a radio frequency (RF) tunable coil have the sample disposed therein, the frequency variation is within a frequency range of an RF resonant frequency of a standard sample of the substance;
determining an impedance frequency variation from the frequency-dependent output signals;
determining an RF frequency variation of at least one characteristic of the substance from the impedance frequency variation;
comparing the RF frequency variation of the at least characteristic of the substance with an RF frequency variation of a corresponding characteristic of a standard sample of the substance, wherein the comparison determines the material content of the sample.

### Claim 2 (depends on 1)

The non-destructive on-line system method of claim 1, wherein the at least one characteristic of the substance is selected from the group consisting of at least one physical characteristic, at least one electrochemical characteristic, at least one chemical characteristic and at least one biological (PPECB) characteristic and any combination thereof.

### Claim 3 (depends on 2)

The non-destructive on-line system method of claim 2, wherein the at least one characteristic comprises either an electrical inductance of the substance or an electrical reactance of the substance.

### Claim 4 (depends on 1)

The non-destructive on-line method of claim 1, wherein the frequency range is approximately ±100 MHz of the resonant frequency.

### Claim 5 (depends on 1)

The non-destructive on-line method of claim 1, wherein the frequency range is approximately from the resonant frequency minus 100 MHz to the resonant frequency plus 100 MHz.

### Claim 6 (depends on 1)

The non-destructive on-line method of claim 1, wherein the material comprises water.

### Claim 7 (depends on 1)

The non-destructive on-line method of claim 1, wherein the output signal comprises either a direct current (DC) voltage signal or an RF voltage signal.

### Claim 8 (depends on 1)

The non-destructive on-line method of claim 1, further comprising optimizing a production process of the sample based on the material content of the sample.

### Claim 9 (depends on 1)

The non-destructive on-line method of claim 1, further comprising
measuring the sample undergoing a modification, the modification is selected from the group consisting of a physical modification, biological modification, chemical modification and any combination thereof; and
controlling a concentration of the sample based on the measurement.

### Claim 10 (depends on 1)

The non-destructive on-line method of claim 1, wherein the substance is selected from the group consisting of tomato puree, tomato ketchup, tomato paste, tomato sauce, tomato beverage, tomato soup, tomato concentrate, apple puree, apple paste, apple sauce, apple beverage, apple concentrate, potato puree, potato paste, potato sauce, potato beverage, potato concentrate.

### Claim 11 (depends on 1)

The non-destructive on-line method of claim 1, further comprising controlling water pollution based on measuring at least one contaminant, the at least one contaminant is selected from organic contaminants, inorganic contaminants and any combination thereof.

### Claim 12 (depends on 1)

The non-destructive on-line method of claim 1, further comprising measuring an acidity parameter in a food product.

### Claim 13 (depends on 1)

The non-destructive on-line method of claim 1, wherein the substance is selected from the group consisting of water-miscible fluids, water-immiscible fluids aggregated solutions, dispersions, emulsions, solution, slurry, polymer, solid and powder and any combination thereof.

### Claim 14 (depends on 1)

The non-destructive on-line method of claim 1, wherein the processor provides a Smith Chart of the impedance frequency variation as a function of the RF frequency and wherein the RF frequency variation of inductance and the RF variation of reactance are determined by use of the Smith Chart.

### Claim 15 (depends on 1)

The non-destructive on-line method of claim 1, wherein the sample comprises either a fluid state or a solid state.

### Claim 16 (depends on 2)

The non-destructive on-line method of claim 2, wherein the physical characteristic is selected from the group consisting of boiling point, refractive index, viscosity, moisture content, rheologic properties, magnetic properties.

### Claim 17 (depends on 2)

The non-destructive on-line method of claim 2, the electrochemical characteristic is selected from conductivity, pH, oxygen content, permittivity permeability, dielectric constant and any combination thereof.

### Claim 18 (depends on 2)

The non-destructive on-line according to claim 2, wherein the chemical parameter is selected from the group consisting of chemical concentration and identity of the composition and any combination thereof.

### Claim 19 (depends on 2)

The non-destructive on-line according to claim 2, wherein the biological parameter is selected from the group consisting of bacteria, mold, fungi, alga, virus, microorganisms, eukaryotes and any combination thereof.

### Claim 20 (depends on 2)

The non-destructive on-line according to claim 2, wherein the sample is further selected from the group consisting of a solid, a sol-gel, a super-critical solution and any combination thereof.
