# US 10,371,620 B2 · Automatic power control liquid particle counter with flow and bubble detection systems

> Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt

- Number: US 10,371,620 B2
- Document ID: US10371620B2
- Status: Granted
- Kind: B2
- Application number: 15/600,418
- Filed: 2017-05-19
- Published: 2017-12-14
- Granted: 2019-08-06
- Earliest claimed: 2016-05-20
- Assignees: Particle Measuring Systems, Inc.
- Applicants: Particle Measuring Systems, Inc.
- Inventors: Brian Knollenberg; Jim Lumpkin; Brett Haley; Matt Soappman; Dan Rodier; Mark Lilly
- Web page: https://patentgrep.com/patent/US10371620B2

## CPC

- G01N 15/1425: {using an analyser being characterised by its control arrangement}
- G01F 1/704: using marked regions or existing inhomogeneities within the fluid stream, e.g. statistically occurring variations in a fluid parameter (G01F1/76, G01F25/00 take precedence)
- G01N 15/0205: by optical means
- G01N 15/06: Investigating concentration of particle suspensions (by weighing G01N5/00; investigating sedimentation of particle suspensions G01N15/04; investigating individual particles G01N15/10)
- G01N 15/1459: {the analysis being performed on a sample stream}
- H05B 47/115: by determining the presence or movement of objects or living beings
- G01N 15/075: by optical means
- G01N 2015/0011: {in liquids, e.g. bubbles}
- G01N 2015/1486: {Counting the particles}
- Y02B 20/40: Control techniques providing energy savings, e.g. smart controller or presence detection
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)
- G01F: MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
- H05B: ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- Y02B: CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO BUILDINGS, e.g. HOUSING, HOUSE APPLIANCES OR RELATED END-USER APPLICATIONS

## Abstract

The systems and methods provided herein relate generally to the improvement of data quality in optical liquid particle counters and control of optical particle counters to achieve longer expected lifetime, for example by avoiding damage caused by electromagnetic radiation and heat. The systems and methods incorporate sensors which characterize the fluid flowing through the flow cell, thereby enhancing accuracy and reducing the number of false positives.

## Claims

### Claim 1

An optical liquid particle counter system comprising:
a liquid particle counter comprising:
a flow chamber for flowing a liquid containing particles along a flow direction through a beam of electromagnetic radiation,
an optical source, in optical communication with said flow chamber, for providing said beam of electromagnetic radiation; and
an optical collection system for collecting and directing at least a portion of electromagnetic radiation onto a photodetector;
wherein said photodetector produces an electric signal characteristic of the number and/or size of said particles detected;
a fluid monitoring system in fluid communication with said flow chamber that detects bubbles in said liquid, a flow rate condition of said liquid, or both bubbles and a flow rate condition;
an actuator for engaging or disengaging an optical interrupter capable of redirecting, reshaping, or reducing the fluence of electromagnetic radiation from said optical source entering said flow chamber; and
a processor in operational communication with said fluid monitoring system and said actuator, wherein said processor receives monitoring data from said fluid monitoring system and provides a control signal to said actuator for engaging or disengaging said optical interrupter;
wherein said processor flags said monitoring data indicative of the presence of bubbles in said liquid as corresponding to a portion of the liquid in said flow chamber, and said control signal comprises timing instructions for actuating said optical interrupter at a time corresponding to passage of said portion of said liquid through said beam of electromagnetic radiation.

### Claim 2 (depends on 1)

The optical liquid particle counter system of claim 1, wherein said control signal is provided by said processor when said processor analyzes said monitoring data and determines the presence of bubbles in said liquid, a flow rate condition of said liquid, or both bubbles and a flow rate condition.

### Claim 3 (depends on 1)

The optical liquid particle counter system of claim 1, wherein said processor receives monitoring data from said fluid monitoring system and provides a control signal to said optical liquid particle counter or a component thereof to increase the power of said optical source to full operational power or to disengage said optical interrupter when said monitoring data indicates the absence of bubbles in said liquid, a normal flow rate condition of said liquid, or both.

### Claim 4 (depends on 3)

The optical liquid particle counter system of claim 3, wherein during startup of said system, said optical liquid particle counter system will not provide power to said optical source until said processor receives said monitoring data from said fluid monitoring system indicating the absence of bubbles in said liquid, a normal flow rate condition of said liquid, or both.

### Claim 5 (depends on 3)

The optical liquid particle counter system of claim 3, wherein said full operational power is greater than or equal to 20 mW, and said normal flow rate is less than or equal to 2000 mL/min.

### Claim 6 (depends on 1)

The optical liquid particle counter system of claim 1, wherein said fluid monitoring system detects bubbles optically, electronically, acoustically, by pressure differential, by density, or a combination thereof.

### Claim 7 (depends on 6)

The optical liquid particle counter system of claim 6, wherein said processor decreases said power of said optical source if said bubble has a diameter greater than or equal to the diameter of the particles being detected.

### Claim 8 (depends on 1)

The optical liquid particle counter system of claim 1, wherein said fluid monitoring system detects a flow rate condition.

### Claim 9 (depends on 8)

The optical liquid particle counter system of claim 8, wherein said flow rate condition is a high flow rate, a low flow rate, a normal flow rate or a flow stoppage.

### Claim 10 (depends on 8)

The optical liquid particle counter system of claim 8, wherein said fluid monitoring system is a differential pressure flowmeter, a transit-time ultrasonic flowmeter, a rotameter/float sensor, a Doppler ultrasonic flow meter, a thermal mass flow meter, an electromagnetic flow meter, a turbine/paddle wheel meter, vortex flow meter, a flow switch, a Coriolis mass flow meter, a CCD or CMOS camera, or a combination thereof.

### Claim 11 (depends on 1)

The optical liquid particle counter system of claim 1, wherein said flow rate condition corresponds to a normal flow rate and said processor provides a control signal to said actuator to disengage said optical interrupter.

### Claim 12 (depends on 1)

The optical liquid particle counter system of claim 1 further comprising:
a liquid conditioner, wherein said liquid conditioner splits a fluid entering said liquid particle counter system into a sampling stream in fluid communication with said flow chamber and a bypass stream and promotes the removal of bubbles out of said sampling stream and into said bypass stream.

### Claim 13 (depends on 12)

The optical liquid particle counter system of claim 12, wherein said liquid conditioner decreases a linear velocity of said liquid within said liquid conditioner with respect to the velocity of said liquid before or after said liquid conditioner.

### Claim 14 (depends on 1)

The optical liquid particle counter system of claim 1, wherein said optical interrupter is a mirror, an optical filter, a polarization optical switch, a shutter, a beam dump, a beam expanding lens, a heat sink or a combination thereof.
