# US 10,368,561 B1 · C. bot prevention in infused coffee

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- Number: US 10,368,561 B1
- Document ID: US10368561B1
- Status: Granted
- Kind: B1
- Application number: 16/002,597
- Filed: 2018-06-07
- Granted: 2019-08-06
- Earliest claimed: 2018-03-06
- Assignees: Kerflummox Holdings, LLC
- Applicants: Janice Benson; Oussama Sabky
- Inventors: Janice Benson; Oussama Sabky
- Web page: https://patentgrep.com/patent/US10368561B1

## CPC

- A23F 5/267: {using additives, specific extraction media or specific coffee blends}
- A23F 5/243: {Liquid, semi-liquid or non-dried semi-solid coffee extract preparations; Coffee gels; Liquid coffee in solid capsules (A23F5/246 takes precedence)}
- B65B 1/00: Packaging fluent solid material, e.g. powders, granular or loose fibrous material, loose masses of small articles, in individual containers or receptacles, e.g. bags, sacks, boxes, cartons, cans, or jars
- B65D 81/2076: {in an at least partially rigid container}
- B65D 81/24: Adaptations for preventing deterioration or decay of contents; Applications to the container or packaging material of food preservatives, fungicides, pesticides or animal repellants (with thermal insulation B65D81/38)
- B67C 7/00: Concurrent cleaning, filling, and closing of bottles; Processes or devices for at least two of these operations
- B65B 29/00: Packaging of materials presenting special problems
- B65B 31/00: Packaging articles or materials under special atmospheric or gaseous conditions; Adding propellants to aerosol containers
- A23F: COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- B65B: MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING (bundling and pressing devices for cigars A24C1/44; devices for tensioning and securing binders adapted to be supported by the article or articles to be bound B25B25/00; applying closure members to bottles, jars or similar containers B67B1/00-B67B6/00; concurrent cleaning, filling and closing of bottles B67C7/00; emptying bottles, jars, cans, casks, barrels or similar containers B67C9/00)
- B65D: CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B67C: CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS

## Abstract

A coffee product including a sealed container having a liquid portion and a headspace. The liquid portion has coffee with a non-oxygen gas dissolved therein and the headspace contains at least approximately 3% oxygen and an amount of a non-oxygen gas. A method of manufacturing the coffee includes dissolving oxygen into a liquid coffee product and packaging the liquid coffee product with oxygen dissolved therein into a sealed container.

## Claims

### Claim 1

A method of manufacturing cold brew coffee comprising:
dissolving oxygen into a liquid coffee product brewed at a temperature less than 50° C. and
packaging said liquid coffee product with oxygen dissolved therein into a sealed container wherein the sealed container has a partial pressure percentage of oxygen of at least approximately 3%.

### Claim 2 (depends on 1)

The method of claim 1, wherein said container is a single use container.

### Claim 3 (depends on 2)

The method of claim 2, wherein said container is a metal can.

### Claim 4 (depends on 1)

The method of claim 1, wherein the container is a bottle.

### Claim 5 (depends on 1)

The method of claim 1, wherein the brew temperature of the liquid coffee product is 3 to 15° C.

### Claim 6 (depends on 1)

The method of claim 1 further comprising:
feeding a coffee product brewed at a temperature less than 50° C. from a vat into the container, wherein between the vat and container, the dissolving step occurs;
dispensing a non-oxygen gas into the container, the non-oxygen gas being a liquid when dispensed; and
sealing the container.

### Claim 7 (depends on 6)

The method of claim 6, wherein the container has a headspace substantially including only oxygen and the non-oxygen gas.

### Claim 8 (depends on 6)

The method of claim 6, wherein the dispensing step is done at a first rate measured in gallons per minute (gpm) and the dissolving step is accomplished by supplying a pressure of oxygen at a second rate measured in positive net pounds per square inch (psi) into an infuser such that the first rate divided by the second rate is a ratio in the range of 0.1-10 gpm/psi.

### Claim 9 (depends on 8)

The method of claim 8, wherein the ratio is 1-5 gpm/psi.

### Claim 10 (depends on 1)

The method of claim 1, wherein after the step of dissolving and prior to the step of packaging, the coffee is recirculated in a holding tank until the coffee having dissolved oxygen therein reaches an oxygen level of 10-40 ppm.

### Claim 11 (depends on 1)

The method of claim 1, wherein the partial pressure percentage of oxygen is less than 10%.

### Claim 12 (depends on 11)

The method of claim 11, wherein a total pressure of a gaseous portion of the sealed container in atmospheres times the partial pressure percentage of oxygen defines a pressure ratio which is 0.03-0.16.

### Claim 13 (depends on 12)

The method of claim 12, wherein the pressure ratio is approximately 0.1125.

### Claim 14 (depends on 6)

The method of claim 6, wherein the non-oxygen gas is nitrogen.

### Claim 15

A cold brew coffee product comprising:
a sealed container comprising a liquid portion and a headspace;
the liquid portion comprising coffee brewed at a temperature less than 50° C. with a non-oxygen gas dissolved therein;
the headspace containing at least approximately 3% oxygen and an amount of the non-oxygen gas.

### Claim 16 (depends on 15)

The product of claim 15, wherein the non-oxygen gas is nitrogen.

### Claim 17 (depends on 15)

The product of claim 15, wherein the headspace has a total pressure between 1-4 atmospheres when the liquid portion is at a temperature of 3° C.

### Claim 18 (depends on 15)

The product of claim 15, wherein the headspace contains approximately 3-6% oxygen.

### Claim 19 (depends on 18)

The product of claim 18, wherein the liquid portion has a pH of 4.6 or greater.

### Claim 20

A method of manufacturing a stable nitrogen infused coffee product comprising the steps of:
dissolving oxygen into a liquid coffee product brewed at temperature less than 50° C.;
packaging the coffee product having dissolved oxygen therein into a container;
dispensing nitrogen into the container to produce a nitrogen infused coffee product; and
sealing the container,
wherein the nitrogen infused coffee product has a pH of 4.6 or greater and remains free of Clostridium botulinum (C. bot) when stored at refrigerated conditions.

### Claim 21 (depends on 20)

The method of claim 20 wherein the pH is 5.0 or greater.

### Claim 22 (depends on 20)

The method of claim 20 wherein the pH is 5.5-6.5.

### Claim 23 (depends on 18)

The product of claim 18 wherein the pH is 5.0 or greater.

### Claim 24 (depends on 18)

The product of claim 18 wherein the pH is 5.5-6.5.

### Claim 25

A cold brew coffee product comprising:
a sealed container comprising a liquid portion and a headspace;
the liquid portion comprising coffee brewed at a temperature less than 50° C. with oxygen and a non-oxygen gas dissolved therein;
the headspace containing oxygen and an amount of the non-oxygen gas;
the liquid portion having a pH of 4.6 or greater wherein the product is free of Clostridium botulinum (C. bot).

### Claim 26 (depends on 25)

The product of claim 25 wherein the pH is 5.0 or greater.

### Claim 27 (depends on 25)

The product of claim 25 wherein the pH is 5.5-6.5.
