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US 10,364,156 B2Granted
Process for producing high grade hydromagnesite and magnesium oxide
AssigneeKarnalyte Resources Inc.
InventorsRobin Phinney, Jonathon Phinney, Siu Ma
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Abstract
The present invention provides a process for producing high purity hydromagnesite from a source of magnesium chloride. The process involves preparation of a magnesium chloride brine of a specific concentration, which is ammoniated at a specific temperature range, followed by carbonation, while maintaining the reaction at a specific temperature range to form a hydromagnesite precipitate. The product can be calcined to generate high purity magnesium oxide compounds.
Claims17
A method of preparing hydromagnesite from a source of magnesium chloride, comprising:
- a) preparing a first brine solution from said source of magnesium chloride, wherein said first brine solution comprises magnesium chloride and calcium chloride;
- b) mixing a sulfate salt into said first brine solution capable of converting said calcium chloride into a calcium sulfate precipitate thereby forming said calcium sulfate precipitate and a second brine solution comprising magnesium chloride;
- c) removing said calcium sulfate precipitate from said second brine solution;
- d) ammoniating said second brine solution, after step c), at a temperature range of about 20° C. to about 60° C. to convert magnesium chloride at least partially into magnesium hydroxide and to form ammonium chloride;
- and
- e) carbonating said magnesium hydroxide while maintaining the reaction temperature at about 20° C. to about 120° C. to form a hydromagnesite precipitate,
- f) wherein said first brine solution contains from about 25% to about 35% by weight magnesium chloride in water,
- g) wherein said mixing of said sulfate salt is carried out at a temperature of about 60° C. to about 90° C.
5 more elements
Dependencies are inferred from the claim text.