Manufacturing method for lithium difluorophosphate powder, and lithium difluorophosphate
AssigneeCentral Glass Company, Limited
InventorsKeita Nakahara, Takayoshi Morinaka, Yuta Ikeda, Natsuya Nishimura
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AssigneeCentral Glass Company, Limited
InventorsKeita Nakahara, Takayoshi Morinaka, Yuta Ikeda, Natsuya Nishimura
Estimating the term…
To provide a manufacturing method with which lithium difluorophosphate powder can be recovered from a lithium difluorophosphate solution. A method for manufacturing lithium difluorophosphate powder is used which includes the steps of precipitating solid lithium difluorophosphate by adding a poor solvent to a solution in which lithium difluorophosphate is dissolved in a main solvent, and obtaining lithium difluorophosphate powder by solid-liquid separation of the solid lithium difluorophosphate from the liquid containing the main solvent and the poor solvent, wherein the relational expression between the octanol/water partition coefficient PP of the main solvent and the octanol/water partition coefficient PA of the poor solvent is defined by the following formula (1). PA≥−4/3×PP+1.2 (1):
A method for manufacturing lithium difluorophosphate powder, comprising the steps of:
Lithium difluorophosphate, wherein 50 mass ppm or greater to 1000 mass ppm or less of at least one selected from the group consisting of n-heptane, toluene, xylene, benezene, and diisopropyl ether is contained.
Dependencies are inferred from the claim text.