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US 10,322,358 B2Granted
Device and method for separating a cyclic diester from polymer melts
AssigneeUhde Inventa-Fischer GmbH
InventorsRainer Hagen, Udo Mühlbauer
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Abstract
The present invention relates to a device and also to a method for separating and recovering a cyclic diester, in particular dilactide or glycolide from polymer melts which include the cyclic diester as impurity. The device and also the method according to the invention allow recovery of the cyclic diester with a high yield and at the same time high purity.
Claims13
A device for separating and recovering a cyclic diester of general Formula I
- R being selected from hydrogen or linear or branched aliphatic radicals with 1 to 6 carbon atoms, from a polymer melt, comprising the diester of general formula I, which comprises
- a) at least one demonomerisation device for removing the diester of general Formula I in gaseous aggregate state from the polymer melt,
- b) at least one separation device, which is connected subsequent to the at least one demonomerisation device and which is in fluidic connection with the at least one demonomerisation device, for separating the diester of general Formula I, in which the diester of general Formula I is converted via a solid into a liquid aggregate state, and
- c) at least one device for producing a vacuum which is connected subsequent to the at least one separation device and which is in fluidic connection with the at least one separation device,
- wherein, subsequent to the at least one device for producing a vacuum, at least one condenser is connected, which is in fluidic connection with an outlet of the at least one device for producing a vacuum,
- wherein, in front of the at least one device for producing a vacuum, at least one device for producing an initial vacuum is connected, which is in fluidic connection with the at least one condenser and/or the at least one device for producing a vacuum;
- and
- wherein the at least one device for producing a vacuum is a cascade of at least two ejector pumps, the cascade of at least two ejector pumps being designed without intermediate condensation.
5 more elements
Dependencies are inferred from the claim text.