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US 10,315,976 B2Granted
Organic compounds
AssigneeGivaudan SA
InventorsAlain Alchenberger, Chloe Berbez, Clare Finn, Dominique Lelievre, Martin Alan Lovchik, Roseline Poignon-Martel, Gilles Romey
Life of this patent
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Abstract
5,9-dimethyl-9-hydroxy-decen-4-al, having the formula (I)
Claims19
A personal care composition, a household care composition or a fine fragrance composition comprising the compound 5, 9-dimethyl-9-hydroxy-decen-4-al, having the formula (I)
A process of forming a personal care composition, a household care composition or a fine fragrance composition, said process comprising the steps of:
- I) reacting hydroxylinalool with ethyl vinyl ether in acid under an inert gas atmosphere at 1 to 100 bar, and a temperature of (−) 10 to 200 degrees centigrade, to form a reaction mixture comprising acetals;
- II) acidifying the cooled reaction mixture at (−20) to 40 degrees centigrade and atmospheric pressure to hydrolyse said acetals;
- III) neutralising the reaction mixture in a base before adjusting the pH of the reaction mixture to a slightly acidic pH of 2 to 7, to yield 5, 9-dimethyl-9-hydroxy-decen-4-al (I);
- and optionally
- IV) distilling the reaction mixture to isolate 5, 9-dimethyl-9-hydroxy-decen-4-al;
- and,
- V) incorporating the isolated 5, 9-dimethyl-9-hydroxy-decen-4-al within the personal care composition, or the household care composition or the fine fragrance composition.
4 more elements
Dependencies are inferred from the claim text.