# US 10,307,705 B2 · Systems for closed loop regeneration of gas dehydration units using liquid petroleum gas

> Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt

- Number: US 10,307,705 B2
- Document ID: US10307705B2
- Status: Granted
- Kind: B2
- Application number: 16/124,263
- Filed: 2018-09-07
- Published: 2019-01-03
- Granted: 2019-06-04
- Earliest claimed: 2017-03-07
- Assignees: Chevron U.S.A. Inc.
- Applicants: Chevron U.S.A. Inc.
- Inventors: Saham Sam Tafreshi; Piyush Balkrishna Shah; Kamalkumar Ishwar Gursahani; Craig Charles Manion
- Web page: https://patentgrep.com/patent/US10307705B2

## CPC

- B01D 53/0438: {Cooling or heating systems}
- B01D 3/14: Fractional distillation {or use of a fractionation or rectification column}
- B01D 3/143: {by two or more of a fractionation, separation or rectification step}
- B01D 5/0057: {in combination with other processes}
- B01D 17/02: Separation of non-miscible liquids
- B01D 17/0214: {with removal of one of the phases}
- B01D 53/261: {by adsorption}
- B01J 20/3408: {of aluminosilicate molecular sieves}
- B01J 20/3475: {in the liquid phase}
- B01D 2253/116: Molecular sieves other than zeolites
- B01D 2256/24: Hydrocarbons
- B01D 2256/245: Methane
- B01D 2257/80: Water
- B01D 2259/4009: using hot gas
- B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28)
- B01J: CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS

## Abstract

A system is disclosed in which water-saturated desiccant in a dehydration unit, having previously been used to dehydrate natural gas, is regenerated in a closed loop process using liquid petroleum gas (LPG). LPG is pumped from a storage tank, vaporized and superheated. The superheated LPG gas enters the dehydration unit such that the hot gas passes over the desiccant thereby regenerating the desiccant. An overhead stream from the dehydration unit passes to a condenser where the temperature of the hot gas from the dehydration unit is dropped to form a fluid stream containing LPG, water and non-condensable gases. The fluid stream passes to a three phase separator for separating the fluid stream into a gas stream, a water stream, and a liquid stream containing LPG which is then returned to the storage tank for reuse in the closed loop process.

## Claims

### Claim 1

A system for regenerating a gas dehydration unit containing saturated mole sieve used in a process for dehydrating a natural gas feed stream, comprising:
a. a storage tank for storing liquid propane and/or butane;
b. a pump for pumping the liquid propane and/or butane from the storage tank;
c. at least two heat exchangers in series for receiving the liquid propane and/or butane and converting the liquid propane and/or butane to a hot propane gas and/or butane gas;
d. a regeneration gas inlet in the gas dehydration unit containing the saturated mole sieve to be regenerated for receiving the hot propane and/or butane gas such that the hot propane gas and/or butane gas passes across the saturated mole sieve thereby regenerating the mole sieve;
e. a condenser in communication with a regeneration gas outlet in the gas dehydration unit for receiving an overhead stream containing the hot propane gas and/or butane gas from the gas dehydration unit and dropping the temperature to form a fluid stream containing liquid propane and/or butane, and containing water and non-condensable gas;
f. a three phase separator in communication with the condenser for separating the fluid stream into a gas stream, a water stream, and a liquid stream comprising liquid propane and/or butane; and
g. a line in communication with the three phase separator for returning the liquid propane and/or butane to the storage tank.

### Claim 2 (depends on 1)

The system of claim 1, further comprising a potassium hydroxide treatment unit located between the three phase separator and the storage tank, wherein the potassium hydroxide treatment unit receives the liquid stream comprising liquid propane and/or butane from the three phase separator for removing hydrogen sulfide, carbonyl sulfide and/or mercaptans from the liquid stream comprising liquid propane and/or butane.

### Claim 3 (depends on 2)

The system of claim 2, further comprising a coalescer located downstream of the potassium hydroxide treatment unit to remove treater waste carryovers.

### Claim 4 (depends on 1)

The system of claim 1, further comprising a distillation column located between the three phase separator and the storage tank, wherein the distillation column removes water, light hydrocarbon gases and C5+ hydrocarbons from the liquid stream comprising liquid propane and/or butane.

### Claim 5 (depends on 1)

The system of claim 1, further comprising a dehydration unit located between the three phase separator and the storage tank, wherein the dehydration unit removes dissolved water from the liquid stream comprising liquid propane and/or butane.