Method for producing chlorosilane gas using continuous tubular reactor
AssigneeLG Chem, Ltd.
InventorsYoo Seok Kim, Jeong Kyu Kim, JinHyoung Yoo, JungWoo Lee, Eunsu Jang
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Abstract
The present invention relates to an apparatus for producing trichlorosilane from tetrachlorosilane in an efficient manner. The apparatus includes an inlet through which reaction raw materials including a metal silicon powder dispersed in liquid tetrachlorosilane enter, a hole through which a gaseous reaction raw material is fed, an outlet through which reaction products including trichlorosilane exit, a tubular reactor in which the reaction raw materials entering through the inlet react with each other during flow, and means for impeding the flow of the fluids to cause collision of the fluids during flow.
Claims9
A method for continuously producing trichlorosilane, comprising:
- reacting a reaction raw material comprising a metal silicon powder dispersed in liquid tetrachlorosilane, with a gaseous reaction raw material, in an apparatus to yield trichlorosilane during flow of the reaction raw material and the gaseous reaction raw material through the apparatus, wherein the apparatus comprises:
- a tubular reactor that is:
- (a) a horizontally-positioned linear tubular reactor containing structures protruding from an inner wall of the tubular reactor to a reaction space that impede the flow of a fluid through the reactor and that cause collision of the fluid during flow of the fluid through the reactor;
- or
- (b) composed of parallel tube segments connected by perpendicular tube segments to form a reactor having a circuitous flow path having a square wave shape with a plurality of right angle bends, whereby each bend impedes flow of fluid through the reactor and causes collision of the fluid during flow of the fluid through the reactor;
- an inlet through which a reaction raw material is introduced into the tubular reactor;
- a cooler connected to the inlet;
- a hole through which a gaseous reaction raw material is fed into the tubular reactor;
- and
- an outlet through which reaction products comprising trichlorosilane exit the tubular reactor.
Dependencies are inferred from the claim text.