# US 10,245,598 B2 · Laboratory centrifuge and method for operating the same with a reversed driving motion of the rotor during acceleration and deceleration

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- Number: US 10,245,598 B2
- Document ID: US10245598B2
- Status: Granted
- Kind: B2
- Application number: 15/088,647
- Filed: 2016-04-01
- Published: 2016-10-06
- Granted: 2019-04-02
- Earliest claimed: 2015-04-02
- Assignees: Sigma Laborzentrifugen GmbH
- Applicants: Sigma Laborzentrifugen GmbH
- Inventors: Michael Sander
- Web page: https://patentgrep.com/patent/US10245598B2

## CPC

- B04B 9/10: Control of the drive; Speed regulating {(for solid bowl screw centrifuges B04B1/2016)}
- B01D 21/262: {by using a centrifuge}
- B04B 5/0414: {comprising test tubes}
- B04B 13/00: Control arrangements specially designed for centrifuges; Program control of centrifuges (control arrangements for feed, charge or discharge B04B11/00)
- B04B: CENTRIFUGES (high-speed drum mills B02C19/11; domestic spin driers D06F; analysing, measuring or monitoring physical or chemical properties of samples during centrifuging, see the relevant subclasses for these procedures, e.g. G01N)
- B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28)

## Abstract

The invention relates to a method for the operation of a laboratory centrifuge (1), wherein a rotor (2) rotates around a horizontal rotational axis (3). It should be avoided that during the start-up of the laboratory centrifuge (1) or the deceleration of the laboratory centrifuge (1) for small angular velocities and small centrifugal forces resulting therefrom due to the gravitational acceleration the product (6) is biased by resulting components of the acceleration in vertical direction which change their sense of direction. For this purpose the acceleration of the rotor (2) is chosen such that when arriving for the first time in a reversing angular position (twelve o'clock position) there is already a centrifugal acceleration being larger than the gravitational acceleration. The corresponding applies for the deceleration of the rotor after the centrifugation.

## Claims

### Claim 1

A method for operating a laboratory centrifuge for centrifuging a product, the laboratory centrifuge comprising a rotor which rotates around a horizontal rotational axis, the product being held at the rotor at a distance of the rotational axis, wherein
a) the rotor is accelerated from a resting angular position, wherein the product is located between a three o'clock position and a six o'clock position and comprises a zero angular velocity, with an acceleration such that when the rotor for a first time arrives at a reversing angular position, wherein the product is located in a twelve o'clock position, the rotor has reached an angular velocity such that a centrifugal acceleration which acts upon the product is larger than a gravitational acceleration,
b) during the acceleration the product passes a six o'clock position and the acceleration from the resting angular position to the first arrival at the reversing angular position is provided over an angle of between 180° to 270° and
c) subsequent to a loading of the product the rotor is transferred with a first sense of rotation from a loading position into the resting angular position from which then the rotor is accelerated with an opposite second sense of rotation towards the reversing angular position.

### Claim 2

A method for operating a laboratory centrifuge for centrifuging a product, the laboratory centrifuge comprising a rotor which rotates around a horizontal rotational axis, the product being held at the rotor at a distance of the rotational axis, wherein
a) the rotor is decelerated from a reversing angular position, wherein the product is located in a twelve o'clock position and comprises an angular velocity such that a centrifugal acceleration acting upon the product is larger than a gravitational acceleration, to an angular velocity of zero for a first arrival in a resting angular position, wherein the product is located between a six o'clock position and a nine o'clock position,
b) during the deceleration the product passes a six o'clock position and the deceleration from the reversing angular position to the first arrival in the resting angular position is provided over an angle of between 180° to 270° and
c) when moving towards the resting angular position during the deceleration the rotor is rotated with a first sense of rotation and there is a subsequent reversing rotation with an opposite sense of rotation from the resting angular position into an unloading position.

### Claim 3 (depends on 1)

The method of claim 1, wherein in the reversing angular position the angular velocity has a magnitude such that the centrifugal acceleration which acts upon the product at least doubles the gravitational acceleration.

### Claim 4 (depends on 2)

The method of claim 2, wherein in the reversing angular position the angular velocity has a magnitude such that the centrifugal acceleration which acts upon the product at least doubles the gravitational acceleration.

### Claim 5 (depends on 1)

The method of claim 1, wherein in the loading position the product is fed to the rotor in an automatized fashion.

### Claim 6 (depends on 2)

The method of claim 2, wherein in the unloading position the product is removed from the rotor in an automatized fashion.

### Claim 7 (depends on 5)

The method of claim 5, wherein with a movement in a same sense of direction the product is
a) fed to the rotor and
b) removed from the rotor after the centrifugation in an automatized fashion.

### Claim 8 (depends on 1)

The method of claim 1, wherein by a balancing device an unbalanced mass of the rotor is reduced or removed, wherein the unbalanced mass of the rotor depends on the mass of the product.

### Claim 9 (depends on 2)

The method of claim 2, wherein by a balancing device an unbalanced mass of the rotor is reduced or removed, wherein the unbalanced mass of the rotor depends on the mass of the product.

### Claim 10 (depends on 1)

The method of claim 1, wherein the product is fixed to the rotor by a mount.

### Claim 11 (depends on 2)

The method of claim 2, wherein the product is fixed to the rotor by a mount.

### Claim 12 (depends on 10)

The method of claim 10, wherein the mount is formed by an accommodating body which forms an accommodation, wherein the product is arranged and which forms a coupling region by which it is possible to fix the accommodation body to the rotor.

### Claim 13 (depends on 11)

The method of claim 11, wherein the mount is formed by an accommodating body which forms an accommodation, wherein the product is arranged and which forms a coupling region by which it is possible to fix the accommodation body to the rotor.

### Claim 14 (depends on 1)

The method of claim 1, wherein a rotational angular position of the rotor is sensed by a sensor and a drive unit of the rotor is controlled on the basis of the sensed rotational angular position.

### Claim 15 (depends on 2)

The method of claim 2, wherein a rotational angular position of the rotor is sensed by a sensor and a drive unit of the rotor is controlled on the basis of the sensed rotational angular position.

### Claim 16 (depends on 1)

A laboratory centrifuge for centrifuging a product, the laboratory centrifuge comprising a rotor, which rotates around a horizontal rotational axis, the product being held at the rotor at a distance of the rotational axis, wherein a drive unit is provided, which is controllable by a control unit comprising control logic for carrying out the method of claim 1.

### Claim 17 (depends on 2)

A laboratory centrifuge for centrifuging a product, the laboratory centrifuge comprising a rotor, which rotates around a horizontal rotational axis, the product being held at the rotor at a distance of the rotational axis, wherein a drive unit is provided, which is controllable by a control unit comprising control logic for carrying out the method of claim 2.

### Claim 18 (depends on 16)

The laboratory centrifuge of claim 16, wherein
a) the rotor forms an accommodation for the product,
b) an input opening of the accommodation is formed on one side of the rotor and
c) a removal opening of the accommodation is formed on the other side of the rotor.

### Claim 19 (depends on 17)

The laboratory centrifuge of claim 17, wherein
a) the rotor forms an accommodation for the product,
b) an input opening of the accommodation is formed on one side of the rotor and
c) a removal opening of the accommodation is formed on the other side of the rotor.

### Claim 20 (depends on 16)

The laboratory centrifuge of claim 16, wherein the drive unit is offset in circumferential direction around the rotational axis with respect to a loading angular position and/or an unloading angular position of the product.

### Claim 21 (depends on 17)

The laboratory centrifuge of claim 17, wherein the drive unit is offset in circumferential direction around the rotational axis with respect to a loading angular position and/or an unloading angular position of the product.

### Claim 22 (depends on 16)

The laboratory centrifuge of claim 16, wherein
a) a sensor is provided for sensing the rotational angular position of the rotor and
b) the control unit comprises control logic which controls the drive unit on the basis of the sensed rotational angular position of the rotor.

### Claim 23 (depends on 17)

The laboratory centrifuge of claim 17, wherein
a) a sensor is provided for sensing the rotational angular position of the rotor and
b) the control unit comprises control logic which controls the drive unit on the basis of the sensed rotational angular position of the rotor.

### Claim 24 (depends on 16)

The laboratory centrifuge of claim 16, wherein the drive unit of the rotor comprises a field-oriented control.

### Claim 25 (depends on 16)

The laboratory centrifuge of claim 16, wherein the drive unit of the rotor comprises a field-oriented control.
