Method for producing a dental prosthesis
AssigneeDENTSPLY SIRONA Inc.
InventorPeter Kreuder
Life of this patent
Estimating the term…
Abstract
A method for producing a dental prosthesis based on lithium silicate glass or lithium silicate glass-ceramic, including the steps of: melting a powder mixture containing at least SiO2, Li2O, Al2O3; producing spherical, lens-shaped or rod-shaped glass particles solidified from the melt; portioning the glass particles and filling them into a crucible; melting the glass particles in the crucible and setting a viscosity v, wherein 4 dPa·s≤v≤80 dPa·s; casting the thus produced melt into a negative mold which is enclosed by an embedding compound and corresponds to the dental prosthesis and; solidifying the melt in the negative mold, and crystallizing lithium metasilicate and/or lithium disilicate from the solidified melt.
Claims16
A method for producing a dental prosthesis based on lithium silicate glass or lithium silicate glass-ceramic, comprising the steps of:
- (a) melting a powder mixture with the composition in wt-%
- SiO2
- 50-70%;
- Li2O
- 5-25%;
- Al2O3
- 0.1-20%;
- K2O
- 0.1-15%;
- CeO2
- 0.1-15%;
- B2O3
- 0-5%;
- P2O5
- 0-15%;
- Tb2O3
- 0-2%;
- ZrO2
- 0-15%;
- ZnO
- 0-4%;
- and
- at least one additive between 0.1 and 5 wt-%, the additive being selected from the group consisting of BaO, CaO, MgO, MnO, Er2O3, Gd2O3, Na2O, Pr2O3, Pr6O11, Sm2O3, TiO2, V2O5, and Y2O3,
- (b) producing spherical or lens-shaped glass particles solidified from the melt;
- (c) portioning the glass particles and filling them into a crucible;
- (d) melting the glass particles in the crucible and setting a viscosity v, wherein 4 dPa·s≤v≤80 dPa·s;
- (e) casting the thus produced melt into a negative mold which is enclosed by an embedding compound and corresponds to the dental prosthesis to be produced;
- (f) solidifying the melt in the negative mold;
- (g) crystallizing lithium metasilicate as main crystalline phase from the solidified melt by employing a first heat treatment at a temperature between 600° C. and 760° C. over a time between 20 min and 120 min, and
- (e) comprising the step of crystallizing lithium disilicate as main crystalline phase in a second heat treatment at a temperature between 760° C. and 860° C. over a time between 5 min and 60 min;
- wherein the first and second heat treatment of the solidified melt takes place either in the negative mold or after removal from the negative mold.
Dependencies are inferred from the claim text.