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US 10,023,496 B1Granted
No fiber calcination of gypsum for gypsum fiberboard
AssigneeUnited States Gypsum Company
InventorYufeng Xu
Life of this patent
Estimating the term…
Abstract
The present disclosure relates to no fiber calcined gypsum and methods of making the same using a multi-stage (typically two-stage) calcination process. The first stage is a high temperature calcination and nucleation stage. The second stage is a lower temperature calcination and crystal growth stage which produces product slurry containing calcined gypsum particles having large, acicular calcined gypsum crystal morphology for use in making gypsum fiberboard.
Claims18
A method comprising:
- performing a first calcination stage comprising heating a first gypsum slurry comprising a first portion of gypsum and a first aqueous fluid to a first temperature in a range of about 270° F. to about 295° F. and under pressure for a sufficient time to convert at least a portion of the first portion of gypsum to a first portion of calcium sulfate hemihydrate and nucleate at least a portion of the first portion of calcium sulfate hemihydrate to form nucleated acicular crystals of a first size, thereby producing a first calcination stage calcined gypsum product slurry having the nucleated acicular crystals of the first size;
- combining in any order a second portion of gypsum and a second aqueous fluid with the first calcination stage calcined gypsum product slurry to form a combined gypsum slurry;
- and
- performing a second calcination stage comprising maintaining the combined gypsum slurry under pressure at a second temperature in the range of about 210° F. to about 240° F. for a sufficient time to form acicular crystals of a second size greater than the first size, thereby forming a second stage calcined gypsum product slurry,
- wherein a final added gypsum amount is a total weight of the first portion of gypsum and the second portion of gypsum,
- wherein a total feed weight is a total weight of the first portion of gypsum, the second portion of gypsum, the first aqueous fluid, and the second aqueous fluid,
- wherein the final added gypsum amount is equal to at most about 50% of the total feed weight, and
- wherein the first portion of gypsum is about 10% to about 50% by weight of the final added gypsum amount.
5 more elements
Dependencies are inferred from the claim text.